TA Instruments

AR1756-0004f

15/03/2013 14:48:55

Sample name	ASW Blank coupon#20 + DI + beads 200rad/s
Sample notes	 
Experiment notes	DI Deionised water, 25 mm diameter. 70 mm total depth of water, 10 mm gap, with PE beads
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1756
Run number	4 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	15/03/2013 14:48:55

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	No
Initial temperature	20.0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:00:30 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	No

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 200.0 rad/s
Duration	0:01:00 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	No

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	20.0 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	0.4094 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0.6 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.261 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	2
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	21.14 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Peak hold step

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0000	199.9	-2129.4	10000	20.0	0.1463	1.000	-694.1	249.9	-2.778	596.0	146.3990	9.546E-3	183.00	18300	3.411E-3	0.0	0.0
2.0000	200.0	350.74	10000	20.0	0.1266	2.000	114.3	250.0	0.4574	515.8	391.0380	8.255E-3	488.80	48880	3.411E-3	0.0	0.0
3.0000	200.0	349.04	10000	20.0	0.1296	3.000	113.8	250.0	0.4551	528.2	554.3710	8.453E-3	692.96	69296	3.411E-3	0.1	0.1
4.0000	200.0	350.18	10000	20.0	0.1272	4.000	114.1	250.0	0.4566	518.3	717.7940	8.293E-3	897.24	89724	3.411E-3	0.1	0.1
5.0040	200.0	341.16	10000	20.0	0.1313	5.004	111.2	250.0	0.4448	534.8	962.7720	8.557E-3	1203.5	1.2035E5	3.411E-3	0.1	0.1
6.0000	200.0	344.93	10000	20.0	0.1292	6.000	112.4	250.0	0.4497	526.6	1126.0100	8.426E-3	1407.5	1.4075E5	3.411E-3	0.1	0.1
7.0000	200.0	338.44	10000	20.0	0.1282	7.000	110.3	250.0	0.4412	522.4	1371.0200	8.359E-3	1713.8	1.7138E5	3.411E-3	0.1	0.1
7.9960	200.0	340.63	10000	20.0	0.1301	7.996	111.0	250.0	0.4441	529.9	1535.7700	8.478E-3	1919.7	1.9197E5	3.411E-3	0.1	0.1
9.0000	200.0	344.83	10000	20.0	0.1282	9.000	112.4	250.0	0.4496	522.4	1780.9600	8.360E-3	2226.2	2.2262E5	3.411E-3	0.2	0.2
10.004	200.0	337.98	10000	20.0	0.1311	10.004	110.2	250.0	0.4406	534.0	1942.7800	8.544E-3	2428.5	2.4285E5	3.411E-3	0.2	0.2
11.000	200.0	331.35	10000	20.0	0.1296	11.000	108.0	250.0	0.4320	528.2	2191.8101	8.451E-3	2739.8	2.7398E5	3.411E-3	0.2	0.2
11.996	200.0	339.34	10000	20.0	0.1250	11.996	110.6	250.0	0.4425	509.2	2351.2600	8.149E-3	2939.1	2.9391E5	3.411E-3	0.2	0.2
13.004	200.0	335.41	10000	20.0	0.1280	13.004	109.3	250.0	0.4373	521.6	2597.0701	8.346E-3	3246.3	3.2463E5	3.411E-3	0.2	0.2
14.000	200.0	335.95	10000	20.0	0.1319	14.000	109.5	250.0	0.4380	537.3	2759.5500	8.597E-3	3449.4	3.4494E5	3.411E-3	0.2	0.2
15.004	200.0	338.30	10000	20.0	0.1266	15.004	110.3	250.0	0.4411	515.8	2923.0801	8.252E-3	3653.9	3.6539E5	3.411E-3	0.3	0.3
16.000	200.0	337.11	10000	20.0	0.1282	16.000	109.9	250.0	0.4395	522.4	3168.0000	8.358E-3	3960.0	3.9600E5	3.411E-3	0.3	0.3
16.996	200.0	339.83	10000	20.0	0.1270	16.996	110.8	250.0	0.4431	517.5	3332.8701	8.280E-3	4166.1	4.1661E5	3.411E-3	0.3	0.3
18.000	200.0	339.11	10000	20.0	0.1290	18.000	110.5	250.0	0.4421	525.8	3579.9299	8.411E-3	4474.9	4.4749E5	3.411E-3	0.3	0.3
18.996	200.0	334.59	10000	20.0	0.1268	18.996	109.1	250.0	0.4362	516.7	3739.8101	8.265E-3	4674.8	4.6748E5	3.411E-3	0.3	0.3
20.008	200.0	338.54	10000	20.0	0.1309	20.008	110.3	250.0	0.4414	533.2	3984.8201	8.531E-3	4981.0	4.9810E5	3.411E-3	0.3	0.3
20.996	200.0	331.79	10000	20.0	0.1311	20.996	108.1	250.0	0.4326	534.0	4148.0601	8.544E-3	5185.1	5.1851E5	3.411E-3	0.3	0.3
22.000	200.0	334.51	10000	20.0	0.1268	22.000	109.0	250.0	0.4362	516.7	4393.9902	8.267E-3	5492.5	5.4925E5	3.411E-3	0.4	0.4
23.000	200.0	333.16	10000	20.0	0.1296	23.000	108.6	250.0	0.4344	528.2	4556.5698	8.451E-3	5695.7	5.6957E5	3.411E-3	0.4	0.4
23.996	200.0	334.57	10000	20.0	0.1282	23.996	109.1	250.0	0.4362	522.4	4719.7598	8.359E-3	5899.7	5.8997E5	3.411E-3	0.4	0.4
25.004	200.0	336.05	10000	20.0	0.1260	25.004	109.5	250.0	0.4382	513.3	4964.9302	8.214E-3	6206.2	6.2062E5	3.411E-3	0.4	0.4
26.000	200.0	335.45	10000	20.0	0.1282	26.000	109.3	250.0	0.4374	522.4	5128.2900	8.359E-3	6410.4	6.4104E5	3.411E-3	0.4	0.4
27.000	200.0	335.42	10000	20.0	0.1240	27.000	109.3	250.0	0.4373	505.1	5373.3599	8.080E-3	6716.7	6.7167E5	3.411E-3	0.5	0.5
28.000	200.0	334.37	10000	20.0	0.1272	28.000	109.0	250.0	0.4360	518.3	5536.6499	8.294E-3	6920.8	6.9208E5	3.411E-3	0.5	0.5
29.000	200.0	337.07	10000	20.0	0.1262	29.000	109.9	250.0	0.4395	514.2	5781.6602	8.227E-3	7227.1	7.2271E5	3.411E-3	0.5	0.5
30.004	200.0	336.93	10000	20.0	0.1286	30.004	109.8	250.0	0.4393	524.1	5944.9399	8.385E-3	7431.2	7.4312E5	3.411E-3	0.5	0.5
31.004	200.0	342.55	10000	20.0	0.1260	31.004	111.7	250.0	0.4466	513.3	6190.0601	8.215E-3	7737.6	7.7376E5	3.411E-3	0.5	0.5
32.000	200.0	336.76	10000	20.0	0.1315	32.000	109.8	250.0	0.4391	535.7	6353.5298	8.571E-3	7941.9	7.9419E5	3.411E-3	0.5	0.5
32.996	200.0	334.42	10000	20.0	0.1272	32.996	109.0	250.0	0.4360	518.3	6599.6802	8.293E-3	8249.6	8.2496E5	3.411E-3	0.5	0.5
33.996	200.0	334.96	10000	20.0	0.1294	33.996	109.2	250.0	0.4367	527.4	6763.6802	8.439E-3	8454.6	8.4546E5	3.411E-3	0.6	0.6
35.004	200.0	333.38	10000	20.0	0.1305	35.004	108.7	250.0	0.4347	531.5	6925.9302	8.504E-3	8657.4	8.6574E5	3.411E-3	0.6	0.6
35.996	200.0	339.31	10000	20.0	0.1268	35.996	110.6	250.0	0.4424	516.7	7171.1001	8.267E-3	8963.9	8.9639E5	3.411E-3	0.6	0.6
37.000	200.0	337.79	10000	20.0	0.1260	37.000	110.1	250.0	0.4404	513.3	7335.2598	8.214E-3	9169.1	9.1691E5	3.411E-3	0.6	0.6
37.996	200.0	342.78	10000	20.0	0.1280	37.996	111.7	250.0	0.4469	521.6	7578.5801	8.345E-3	9473.2	9.4732E5	3.411E-3	0.6	0.6
38.996	200.0	338.26	10000	20.0	0.1282	38.996	110.3	250.0	0.4410	522.4	7741.8501	8.358E-3	9677.3	9.6773E5	3.411E-3	0.6	0.6
40.004	200.0	334.45	10000	20.0	0.1288	40.004	109.0	250.0	0.4361	524.9	7986.9800	8.400E-3	9983.7	9.9837E5	3.411E-3	0.7	0.7
40.996	200.0	335.50	10000	20.0	-0.1075	40.996	109.4	250.0	0.4374	-438.1	8150.3501	-7.009E-3	10188	1.0188E6	3.411E-3	0.7	0.7
42.000	200.0	336.95	10000	20.0	0.1286	42.000	109.8	250.0	0.4393	524.1	8396.2998	8.385E-3	10495	1.0495E6	3.411E-3	0.7	0.7
42.996	200.0	325.36	10000	20.0	0.1250	42.996	106.1	250.0	0.4242	509.2	8558.6602	8.147E-3	10698	1.0698E6	3.411E-3	0.7	0.7
43.992	200.0	337.55	10000	20.0	0.08481	43.992	110.0	250.0	0.4401	345.5	8722.0898	5.530E-3	10903	1.0903E6	3.411E-3	0.7	0.7
45.004	200.0	343.38	10000	20.0	0.1260	45.004	111.9	250.0	0.4477	513.3	8967.0596	8.214E-3	11209	1.1209E6	3.411E-3	0.8	0.8
45.996	200.0	338.27	10000	20.0	0.1280	45.996	110.3	250.0	0.4411	521.6	9131.4902	8.347E-3	11414	1.1414E6	3.411E-3	0.8	0.8
46.996	200.0	331.10	10000	20.0	0.1305	46.996	107.9	250.0	0.4317	531.5	9375.4902	8.503E-3	11719	1.1719E6	3.411E-3	0.8	0.8
47.996	200.0	329.51	10000	20.0	0.1286	47.996	107.4	250.0	0.4296	524.1	9538.7803	8.384E-3	11923	1.1923E6	3.411E-3	0.8	0.8
48.996	200.0	335.17	10000	20.0	0.1296	48.996	109.2	250.0	0.4370	528.2	9783.8301	8.453E-3	12230	1.2230E6	3.411E-3	0.8	0.8
50.004	200.0	335.86	10000	20.0	0.1248	50.004	109.5	250.0	0.4379	508.4	9947.1797	8.135E-3	12434	1.2434E6	3.411E-3	0.8	0.8
51.000	200.0	343.76	10000	20.0	0.09069	51.000	112.0	250.0	0.4482	369.5	10192.200	5.913E-3	12740	1.2740E6	3.411E-3	0.9	0.9
51.996	200.0	348.03	10000	20.0	0.1747	51.996	113.4	250.0	0.4538	711.7	10357.000	0.01139	12946	1.2946E6	3.411E-3	0.9	0.9
52.996	200.0	343.94	10000	20.0	0.1294	52.996	112.1	250.0	0.4484	527.4	10603.100	8.439E-3	13254	1.3254E6	3.411E-3	0.9	0.9
53.996	200.0	323.60	10000	20.0	0.3837	53.996	105.5	250.0	0.4219	1563	10763.900	0.02501	13455	1.3455E6	3.411E-3	0.9	0.9
55.004	200.0	341.16	10000	20.0	0.1268	55.004	111.2	250.0	0.4448	516.7	10928.700	8.267E-3	13661	1.3661E6	3.411E-3	0.9	0.9
55.996	200.0	339.37	10000	20.0	0.1327	55.996	110.6	250.0	0.4425	540.6	11174.100	8.651E-3	13968	1.3968E6	3.411E-3	0.9	0.9
56.996	200.0	336.10	10000	20.0	0.1307	56.996	109.6	250.0	0.4382	532.4	11336.300	8.518E-3	14170	1.4170E6	3.411E-3	0.9	0.9
57.996	200.0	340.24	10000	20.0	0.1339	57.996	110.9	250.0	0.4436	545.6	11580.700	8.730E-3	14476	1.4476E6	3.411E-3	1.0	1.0
59.000	200.0	340.32	10000	20.0	0.1260	59.000	110.9	250.0	0.4437	513.3	11744.000	8.213E-3	14680	1.4680E6	3.411E-3	1.0	1.0
59.992	200.0	332.35	10000	20.0	0.1272	59.992	108.3	250.0	0.4333	518.3	11989.100	8.292E-3	14986	1.4986E6	3.411E-3	1.0	1.0

